By subjecting a material to frictional forces over several cycles, material is removed from a controlled location. After sufficient cycles, enough material has been removed from the sample surface to have a measurable difference from its original state. The wear track produced from the reciprocating wear test can be analyzed under methods like scanning probe microscopy to retrieve material loss through wear. Reciprocating wear analysis can give an estimation of the useful life of a material by measuring the material removal rate. Reciprocating wear testing is useful for analyzing very small amounts of material removal like thin film coatings.

Typical Experimental Results:

wear4

SPM image of wear track created through reciprocating wear testing

wear 5

Line profile across the wear track created through reciprocating wear testing

Wear Rate of Hard Drive Disc after 700 and 1000 Passes

Passes Average Cross Sectional Area (µm^2) Wear Volume (µm^3) Wear Rate (m^3/N*m)
700 0.316 3160 2.30*10-15
1000 0.441 4410 2.25*10-15

Applications:

 Abrasive Wear  Adhesive Wear Bio Materials
Bulk Metals Coatings Engineered Surfaces
High Temperature Test Lifetime Cycle Load Effect
Liquid Lubrication Material Removal Rate Reciprocating Wear
Scuffing Scratching Solid Lubrication
Thin Films Variable Load Variable Speed
Wafers Wear Rate Wear Volume

 

For more information please read our application notes:
Light Load Reciprocating Wear of Computer Hard Disk Coatings

 

Instruments: The Tribometer TS 501

triboster

Key Specifications:

Detecting Range 0-500gf (4.9N) Friction Force
Friction Coefficient Resolution 0.001
Max Sample Size 178x60x50mm
Measurement Speed 0.2-11mm/s
Measurement Stroke 1-80mm
Max Tempterature 200 degrees C

 

Light Load Reciprocating Wear of Computer Hard Disk Coatings

 

With computers having a large role in daily life, it is important to protect the hard drive as much as possible to minimize the risk of data loss. Hard drive manufacturers implement techniques such as take-off and landing zones for the head slider as well as magnetic locks for the actuator arm to help protect the hard drive. Even with such precautions, unexpected shock or vibration can cause the head to contact the hard drive platter, causing damage to magnetic recording layer on the disk. To prevent this, lubrication and diamond-like carbon (DLC) coatings are applied to the hard disk surface to protect the magnetic layer from crash damages and frictional wear.

 

Because both the lubrication layer and DLC coatings are on the order of tens of nanometers in thickness and the head slider is a very small and light device, thus, wear study of these coatings requires light contact loads and high sliding speeds. Ebatco NAT Lab’s TS-501 tribometer made by Kyowa is capable of carrying out such a challenging task. The TS-501 can operate under 5-500gf load at a speed up to 100mm/second in order to create a reciprocating wear track on the platter surface. The reciprocating wear test may be performed up to hundreds or even thousands of cycles along a single wear track. With the ability to use wear counterparts of different contact formats as well as to perform tests at light loads and a large number of cycles, the TS-501 is an excellent choice for evaluating the wear resistance and durability of the hard disk platter.

 

The data presented here is for a hard disk platter that underwent reciprocating wear tests using the TS-501. A sapphire ball of 3mm in diameter was used as the wear counterpart. A 10 mm stroke length, 20 gf load, 5mm/second sliding speed, and 700 or 1000 cycles were used for the wear tests. After the wear tests, three segments from each wear track were analyzed using scanning probe microscopy in order to determine the cross-sectional area of the wear tracks. From the cross sectional area and the stroke length, the wear volumes were determined. Knowing the wear volume, force and total sliding distance yields the wear rate of the hard disk platter under the selected wear testing conditions.

 

AppNote-34

 

AppNote-35

 

AppNote-36

 

As exemplified above, light load, high speed reciprocating wear analysis is a very useful and effective approach to evaluate wear resistance and durability of ultra thin films, coatings and bulk material surfaces used in applications where contact force is low and sliding speed is high. These applications may include electrical switches, printer heads, printing papers, flooring materials, touch screens on electronics, and light load ball bearings.

 

ASTM Number Title Website Link
G163-10 Standard Guide for Digital Data Acquisition in Wear and Friction Measurements Link
G203-10 Standard Guide for Determining Friction Energy Dissipation in Reciprocating Tribosystems Link

 

ISO Number Title Website Link
20808 Fine ceramics (advanced ceramics, advanced technical ceramics)– Determination of friction and wear characteristics of monolithic ceramics by ball-on-disc method Link