Modulus mapping is a technique to map and display the mechanical properties of a material surface through joint actions of dynamic mechanical testing (nanoDMA) and in-situ SPM (scanning probe microscopy) imaging. A high frequency sinusoidal force is applied to the indenter probe while it is being raster scanned over a sample surface. The resultant displacement of the indenter probe at each pixel position then is analyzed for amplitude and phase lag from the dynamic force input signal. As a result, storage modulus, loss modulus and tangent delta of the material surface are quantified at each pixel position and displayed in a colored image.
Because of the inherited sensitivities of the nanoscale dynamic mechanical testing and scanning probe microscopy incorporated in the technique, modulus mapping has shown promises and advantages in rapidly characterizing and visualizing variation of mechanical properties at nanoscale over grain boundaries, interfaces, inter-phases, multiphase or multilayer composites, precipitates, and additives.


Typical Experimental Results

Modulus mapping combined for complex modulus, loss modulus, and storage modulus

Modulus Mapping of Metal-Coating Interface on partially coated wire

Line profile of complex modulus

Complex Modulus Line Profile


Applications

AlloysComposite MaterialsCopolymers
Dynamic Mechanical AnalysisGrain BoundariesHeterogeneous Structures
InterfacesInter-PhasesMechanical Property Mapping
Modulus MappingMulti-LayersMulti-Phases
NanomaterialsPhase ImagePolymer Blend
PrecipitatesReinforced MaterialsScanning Probe Microscopy
SteelsStorage and Loss ModulusTangent Delta

Instrument: Multi-Technique and Full-Feature Nanoindentation System

Multi-Technique and Full-Feature Nanoindentation System in laboratory
Multi-Technique and Full-Feature Nanoindentation System with indenter tip, transducer, optics, and stage

Instrument Key Specifications

Temperature Range5 to 300 °C
Displacement Resolution0.02 nm
Force Range30 nN to 10 mN
Force Resolution1 nN
Frequency Range1 to 300 Hz
AtmosphereOpen Air, Inert Gas